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Comprehensive evolved gas analysis of amorphous precursors for S-doped titania by in situ TG–FTIR and TG/DTA–MSPart 1. Precursor from thiourea and titanium(IV)-isopropoxide

Journal of Analytical and Applied Pyrolysis, no. 2 (2008): 292-297

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Abstract

Decomposition of an amorphous precursor for S-doped titania (TiO2) nanopowders, prepared by controlled sol–gel hydrolysis–condensation of titanium(IV) tetraisopropoxide and thiourea in aqueous isopropanol, has been studied up to 800°C in flowing air by simultaneous thermogravimetric and differential thermal analysis coupled online with qu...More

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