Synthesis and characterization of a new class of heteronuclear derivatives of zirconium(IV)

Nandu Bala Sharma,Anirudh Singh,Ram C. Mehrotra

Transition Metal ChemistryCoord. Chem. Rev.Chem. Rev.Chem. Soc. Rev.Chem. Rev .Prog. Inorg. Chem.PolyhedronChem. Rev.AnalystJ. Indian Chem. Soc.Transition Met. Chem.Synth. React. Inorg. Met. Org. Chem.（2005）

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摘要

Reactions of Zr{Al(OPri)4}2Cl2 or Zr{Nb(OPri)6}2Cl2 with KNb(OPri)6/KAl(OPri)4 and diethanolamines RN(CH2CH2OH)2 [R=H(LHH2), Me(LMeH2), and Ph(LPhH2)] in the presence of two equivalents of Et3N yield interesting hetero(bi- and tri-) nuclear derivatives (1)–(8) All of these new derivatives have been characterized by elemental analyses, molecular weight measurements, and spectroscopic studies.

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关键词

Molecular Weight,Physical Chemistry,Zirconium,Inorganic Chemistry,Catalysis

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