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High specific activity steroids II: Microscale synthesis of norgestrel-[9,11-3H]

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, no. 12 (1992): 995-1003

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Abstract

The synthesis of the high specific activity (39 Ci/mmole) tritium labelled steroid norgestrel is described. A practical synthesis of the required substrate for tritium incorporation, 18-methyl-DELTA9(11)-estradiol-3-methyl ether (6), was developed from norgestrel itself. Following reduction with carrier-free tritium gas, microscale condit...More

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