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Study of zinc thiocarbamide chloride, a single-source precursor for zinc sulfide thin films by spray pyrolysis

Journal of Thermal Analysis and Calorimetry, no. 2 (2004): 497-506

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Abstract

Thermal decomposition of the title compound, Zn(tu)2Cl2 (tu=thiourea), was studied up to 1200°C in dynamic inert (N2) and oxidative (air) atmospheres using simultaneous TG/DTA techniques. In addition, XRD and IR were employed ex situ to resolve the reaction mechanism and products. Cubic ZnS (sphalerite) is formed below 300°C in both atmo...More

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