S(3) HMBC: Spin-State-Selective HMBC for accurate measurement of homonuclear coupling constants. Application to strychnine yielding thirteen hitherto unreported JHH.

Louise Kjaerulff,Andrew J Benie,Casper Hoeck,Charlotte H Gotfredsen,Ole Winneche Sorensen

Journal of Magnetic Resonance（2016）

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摘要

•S3 HMBC is a novel way of measuring homonuclear coupling constants and their signs.•Application of S3 HMBC to strychnine led to thirteen hitherto unreported JHH.

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关键词

S3 HMBC,HMBC,RDC,J coupling constants,Small molecules

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