What is the absolute configuration of (+)-crispatanolide isolated from Makinoa crispata (liverwort)?

Katsuyuki Nakashima,Hiroyuki Kawano, Minako Kumano,Hikari Kodama, Masayo Kameoka, Akiyo Yamamoto,Reiko Mizutani,Masakazu Sono,Motoo Tori

Tetrahedron Letters（2015）

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摘要

•Absolute configuration of (+)-crispatanolide (liverwort sesquiterpenoid) was established.•(+)-Crispatanolide possessed ent-cycloeudesmane skeleton.•Chirality introduction was done by CBS reduction of 3-substituted-2-bromocyclohex-2-en-1-one.

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关键词

Crispatanolide,Absolute configuration,Cycloeudesmane,Synthesis

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