Activation of TEMPO by ClO 2 for oxidation of cellulose by hypochlorite-Fundamental and practical aspects of the catalytic system.

Timo Pääkkönen,Raili Pönni,Jinze Dou,Markus Nuopponen,Tapani Vuorinen

Carbohydrate Polymers（2017）

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摘要

•TEMPO can be rapidly activated with ClO2 without bromide addition.•Oxidation of primary alcohols is not dependent on the activation method of TEMPO.•Oxidation of secondary alcohols can be avoided with exclusion of bromide.

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关键词

2,2,6,6-Tetramethyl-1-piperidinyloxy (PubChem CID: 2724126),Chlorine dioxide (PubChem CID: 24870),Sodium hypochlorite (PubChem CID: 23665760),Sodium chlorite (PubChem CID: 23668197),Sodium hydroxide (PubChem CID: 14798),Hydrochloric acid (PubChem CID: 313)

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