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Large multiresidue analysis of pesticides in edible vegetable oils by using efficient solid-phase extraction sorbents based on quick, easy, cheap, effective, rugged and safe methodology followed by gas chromatography-tandem mass spectrometry.

Journal of Chromatography A(2016)

引用 71|浏览24
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摘要
•Multiresidue method for edible vegetable oils using GC–MS/MS.•Evaluation of different sorbents for the clean-up step using QuEChERS methodology.•Comparison of the novel EMR-Lipid sorbent with Z-Sep and PSA.•Procedural Standard Calibration to correct recovery losses.•Several pesticides are detected in most of the olive oil samples.
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关键词
GC–MS/MS,Edible vegetable oils,Multiresidue pesticide analysis,Procedural Standard Calibration,EMR-Lipid
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