Dynamic Viscoelasticity of PUF under Small Strain and Prediction of Dynamic Viscoelasticity in a Wide Frequency Range
Journal of applied polymer science(2018)
摘要
ABSTRACTThe dynamic viscoelasticity of polyurethane fiber (PUF) under small strain was studied with dynamic mechanical analysis and differential scanning calorimetry, and its viscoelasticity was predicted in a wide frequency range. The results revealed that the loss factor (tan δ) was about 0.05 and the phase angle (δ) was 2.86°, very close to the δ of a perfect elastomer in the range from −100°C to −80°C. The master curves superimposed by time‐temperature superposition (TTS), the frequency range of the storage modulus master curve spanned 17 orders of magnitude from 10−7 Hz to 1010 Hz, and the loss modulus master curve spanned 13 orders of magnitude from 10−3 Hz to 1010 Hz. The apparent activation energy of the soft segment relaxation decreased with increasing temperature in the range from −70 to −26°C. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019, 136, 47070.
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关键词
apparent activation energy,dynamic viscoelasticity,loss modulus,PUF,storage modulus
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