Self-assembly of copper-free maltoheptaose-block-polystyrene nanostructured thin films in real and reciprocal space.

Yingjie Liao,Laurent J Goujon,Eric Reynaud,Sami Halila,Alain Gibaud,Bin Wei,Redouane Borsali

Carbohydrate Polymers（2019）

引用 9|浏览17

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摘要

•Copper nanopowder catalyst made removal of residual copper easy after click reaction.•Improved synthetic method also help scale up the synthesis of copper-free MH-b-PS.•The microphase separation of MH-b-PS was investigated by AFM, SAXS and GISAXS.•The phase of MH-b-PS transited from Hex to Bcc when changing the annealing solvent.

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关键词

Carbohydrate-based block copolymers,Microphase separation,Grazing incidence small angle X-ray scattering,Solvent vapor annealing,Copper-catalyzed azide-alkyne cycloaddition

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