Three-component coupling of acetylenic sulfones, Grignard reagents and α, β-unsaturated carbonyls: A convenient synthesis of diallylic alcohols

Changqing Liu,Chao Zha,Jing Jia,Jian Fan,Zhenda Liang, Zhengchun Yin,Ying Sun,Meihua Xie

Journal of Organometallic Chemistry（2016）

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摘要

A convenient synthesis of diversely substituted diallylic alcohols is developed via Cu-mediated three-component coupling reaction of acetylenic sulfones, Grignard reagents and α, β-unsaturated carbonyls. Polysubstituted diallylic alcohols containing a sulfonyl group could be obtained in up to 85% yield.

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关键词

Acetylenic sulfone,Grignard reagent,α, β-unsaturated carbonyl,Diallylic alcohol

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