Synthesis of Nitriles from Aldehydes with Elongation of the Molecule with Two Carbon Atoms
European journal of organic chemistry(2018)
摘要
A new protocol for the synthesis of nitriles from carbonyl compounds with elongation of the molecule with two carbon atoms was developed. It involves a reaction of ethyl cyanoacetate with different aldehydes in the presence of iron pentacarbonyl as a reducing agent. This protocol is very simple and requires only commonly available reagents, with no catalyst or complicated ligands being employed.
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关键词
Aldehydes,Nitrile,Iron carbonyl,CO surrogate,Reductive alkylation,Reduction,Carbonyl ligands
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