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Effect of pH in the hydrothermal preparation of monoclinic tungsten oxide

Journal of Solid State Chemistry, (2020): 121044

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Abstract

This paper presents the preparation of monoclinic WO3 by a one-step hydrothermal method. The effect of very acidic pH (0.1) and the significance of various additives (CH3COOH, NaClO4, Na2SO4) were investigated. To clarify the role of pH on the obtained crystal structure and morphology, every synthesis using pH 1 were repeated, and the eff...More

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