High-throughput planar solid-phase extraction coupled to orbitrap high-resolution mass spectrometry via the autoTLC-MS interface for screening of 66 multi-class antibiotic residues in food of animal origin

Annabel Mehl, Lena J Schmidt, Laszlo Schmidt,Gertrud E Morlock

Food Chemistry（2021）

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摘要

•HTpSPE-autoTLC-HESI-HRMS screening developed for 66 antibiotics of nine classes.•The autoTLC-MS interface allowed automated zone elution via simple clicks on target zones.•HTpSPE was directly coupled to orbitrap high-resolution mass spectrometry.•As proof-of-principle, the method was validated according to EU requirements.

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关键词

High-throughput planar solid-phase extraction,Clean-up,Veterinary antibiotic residues,Automated TLC-MS interface,Orbitrap high-resolution mass spectrometry,Variable data-independent acquisition

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