Investigating the chemical impurity profiles of fentanyl preparations and precursors to identify chemical attribution signatures for synthetic method attribution

Simon P B Ovenden,Lyndal J McDowall,Hugh E McKeown,Nathan W McGill,Oliver A H Jones,James R Pearson, Marija Petricevic, Michael L Rogers,Trevor J Rook,Jilliarne Williams,Renée L Webster,Shannon D Zanatta

Forensic Science International（2021）

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摘要

•Determining method of production is of benefit to investigative agencies.•Identifying chemical attribution signatures aids synthetic production determination.•Janssen and Siegfried acylation methods for fentanyl production were investigated.•Different methods of 4-anilino-N-phenethylpiperidine (ANPP) also investigated.

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关键词

Chemical attribution signatures,Chemical forensics,Impurity profiling,Fentanyl,Method attribution,LC-HRMS

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