Synthesis of α-CF3-substituted γ,δ-didehydro lysine derivatives

Anna N. Philippova,Daria V. Vorobyeva,Tamara P. Vasilyeva,Artur K. Mailyan,Pavel S. Gribanov,Sergey N. Osipov

Mendeleev Communications（2022）

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摘要

An efficient and selective access to novel α-CF3-substituted γ,δ-didehydro lysine derivatives and their phosphorus analogues has been developed via the Cu-catalyzed Mannich reaction of α-amino α-propargyl α-trifluoromethyl carboxylates or phosphonates with different secondary amines and paraformaldehyde.

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关键词

α-amino carboxylates,α-amino phosphonates,Mannich reaction,γ,δ-didehydro lysine,hydrogenation

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