A method for determining valproic acid in human whole blood and urine via gas chromatography-mass spectrometry and small-scale inter-laboratory trial

Akira Namera,Kyoko Uekusa,Takeshi Saito,Kanji Yoshimoto,Naoki Ishiuchi,Kazuhiro Murata,Masataka Nagao

Legal Medicine（2022）

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摘要

•A simple and cost-effective analysis of valproic acid in whole blood and urine.•Valproic acid in the extracted solution was derivatized by trimethylsilyl diazomethane.•Inter laboratory testing showed good agreement between sets of data.

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关键词

Valproic acid,Trimethylsilyldiazomethane,Whole blood,Urine,GC-MS

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