Overcoming challenges in ⁶⁷Zn NMR: a new strategy of signal enhancement for MOF characterization

Wanli Zhang,Alia Hassan,Jochem Struppe,Martine Monette,Ivan Hung,Zhehong Gan,Vinicius Martins,Victor Terskikh,Yining Huang

CHEMICAL COMMUNICATIONS（2023）

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摘要

Zn-67 solid-state NMR suffers from low sensitivity, limiting its ability to probe the Zn2+ surroundings in MOFs. We report a breakthrough in overcoming challenges in Zn-67 NMR. Combining new cryogenic MAS probe technology and performing NMR experiments at a high magnetic field results in remarkable signal enhancement, yielding enhanced information for MOF characterization.

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nmr,signal enhancement

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Overcoming challenges in 67Zn NMR: a new strategy of signal enhancement for MOF characterization

Overcoming challenges in ⁶⁷Zn NMR: a new strategy of signal enhancement for MOF characterization