Visible light promoted and chlorophyll catalyzed α-oxidation of amines to amides under aerobic conditions: Synthesis of 3,4-dihydroisoquinolin-1(2H)-ones and N-phenyl oxalamides

Jingxuan Zhang,Kang Li,Lin Wang,Lei Huang,Haoyi Zhou,Yisong Liu,Hongqi Xie,Jianguo Zeng,Pi Cheng

Tetrahedron Letters（2023）

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摘要

A visible-light-promoted α-oxidation of amines to amides is reported. Natural pigment chlorophyll is used as photosensitizer to generate singlet molecular oxygen 1O2 as oxidants.

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关键词

Chlorophyll, Visible-light photoredox, Oxidation, Amides, Isoquinolines, Oxamides

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