Organoiodine-mediated Dehydrogenative N–N Coupling of Aryl Alkoxycarbamates
Tetrahedron(2023)
摘要
An environmentally benign and efficient approach has been developed for the construction of corresponding N–N coupled dialkoxyhydrazines in good yields (up to 91%) via phenyliodine diacetate (PIDA) mediated oxidative dimerization of alkoxycarbamates. The advantages of this transformations are mild conditions, functional-group tolerance and operationally simple. Notably, the cross-coupling of two different aryl alkoxycarbamates is also demonstrated, which provides a straightforward method to structurally complex N–N molecules.
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关键词
Hypervalent iodine,Oxidation,N -N coupling,Aryl alkoxycarbamates,Phenylamide derivatives
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