Solvent-free reaction of 4-amino-1,2,4-triazole-3-thioles with 1,2,4-triazine-5-carbonitriles

Ya. K. Shtaitz, E. D. Ladin, E. S. Il’inykh, E. S. Starnovskaya, D. S. Kopchuk, G. V. Zyryanov,V. L. Rusinov

Russian Chemical Bulletin（2024）

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摘要

A solvent-free reaction of 5-cyano-1,2,4-triazines with 4-amino-1,2,4-triazole-3-thiols was studied. The reactions take place only at elevated temperature (200 °C) and unexpectedly produce 5-amino-1,2,4-triazines in the yields up to 36

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关键词

1,2,4-triazine-5-carbonitriles,4-amino-1,2,4-triazole-3-thiols,nucleo-philic ipso-substitution,5-amino-1,2,4-triazines

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