Hydrothermal synthesis of iron titanate hexagonal nanoplates for electrochemical detection of nitrofurazone

Microchimica Acta(2024)

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摘要
An electrochemical sensor is established using an iron titanate (FeTiO3) modified glassy carbon electrode (GCE) to detect nitrofurazone. Various microscopic and spectroscopic analysis was performed to reveal the properties of the prepared FeTiO3 hexagonal nanoplates. The FeTiO3/GCE presents enhanced electrochemical response to nitrofurazone at the peak reduction potential of − 0.471 V with a larger peak current than the bare GCE due to high electrical conductivity, enhanced specific surface area, and abundant active sites. The superior nitrofurazone detection performance includes the low limit of detection of 0.002 μM and the sensitivity of 0.551 µA µM−1 cm−2 in the linear concentration range of 0.01–162.2 μM. The reproducibility and selectivity studies of the FeTiO3/GCE show excellent results with a relative standard deviation of < 5
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关键词
Iron titanate,Perovskite,Hydrothermal synthesis,Modified glassy carbon electrode,Nitrofurazone,Nitrofural,Antibiotics
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