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New Au(III), Pt(II) and Pd(II) complexes with glycyl-containing homopeptides

JOURNAL OF COORDINATION CHEMISTRY(2008)

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Abstract
Twelve new Au(III), Pt(II) and Pd(II) complexes with glycyl-containing homopeptides glycyl-glycine (G2), glycyl-glycyl-glycine (G3), glycyl-glycyl-gycyl-glycine (G4), glycyl-glycyl-glycyl-glycyl-glycine (G5) and glycyl-glycyl-glycyl-glycyl-glycyl-glycine (G6) have been synthesized, isolated and characterized spectroscopically and structurally by means of solid-state linear-dichroic infrared (IR-LD) spectroscopy of oriented colloids in nematic liquid crystal host, H-1- and C-13-NMR, TGA and DSC, UV-Vis spectroscopy, EPR, ESI- and FAB mass spectrometry and HPLC tandem mass spectrometry (HPLC-MS/MS). Quantum chemical calculations are carried out with a view to obtain the structures and spectroscopic properties of the ligand and newly synthesized metal complexes.
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Key words
Glycyl-containing homopeptides,Au(III),Pd(II),Pt(II),Cisplatin,Complexes,Solid-state linear polarized IR-spectroscopy,UV-Vis,EPR,Quantum chemical calculations,H-1- and C-13 NMR,ESI MS,TGA and DSC,HPLC-MS-MS
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