A Cautionary Tale in Decanolide Synthesis
SYNLETT（2008）
摘要
An efficient convergent approach to the synthesis of the novel dioxolenone alcohol 3 is described and on thermolysis of 3 a macrodiolide, 12, was obtained via an intermediate P-acyl ketene. Macrodiolide 16 was obtained on thermolysis of the known dioxolenone alcohol 2 rather than the decanolide, diplodialide A.
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关键词
decarestrictines,polyketides,dioxolenones,cyclisation,dimerisation
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