Sub-ambient and Medium Temperature Calibration
Journal of thermal analysis(1993)
Abstract
With some attention to temperature calibration but no other special precautions the temperatures of both solid-solid and melting transitions can be determined to within a few tenths of a Kelvin of absolute values in a range of heat-flux and power-compensation DSC instruments. Materials showing several solid-solid transitions are potentially useful multiple calibrants but require some work to define appropriate thermal treatments that lead to reproducible behaviour.
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Key words
DSC,melting transitions,reproducible behaviour,solid-solid transitions,temperature calibration
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