New Protocol for Masking and Unmasking Vicinal Hydroxyl and Formyl Groups in 6-Hydroxyarene-1,3-dicarboxaldehydes

SYNTHETIC COMMUNICATIONS(2009)

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摘要
A simple and efficient protocol is revealed for the masking and unmasking of an -hydroxyl benzaldedyde group in aromatic dialdehydes by forming keto-enamine Schiff bases and subsequent unmasking using NaN3/DMF.
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关键词
Enamine,2-hydroxy benzaldehydes,masking,NMR spectroscopy,regioselectivity,Schiff bases,unmasking
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