Synthesis of a new pentanuclear gold cluster by metal evaporation. Preparation and X-ray structure determination of [tris{bis(diphenylphosphino)methane}][bis(diphenylphosphino)methanido]pentagold dinitrate

Jan W. A. van der Velden,Jan J. Bour,Frans A. Vollenbroek,Paul T. Beurskens,Jan M. M. Smits

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS（1979）

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摘要

The evaporation of metallic gold into an ethanolic solution of bis(diphenylphosphino)methane (dppmH) and NH4NO3 results in the formation of [Au5(dppmH)3(dppm)](NO3)2 with (dppm)=[Ph2PCHPPh2]–; X-ray structure analysis reveals the presence of an Au–C bond.

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methane

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