[HSO3-pmim][CH3SO3] as an efficient catalyst for chemoselective synthesis of 1,1-diacetates under ultrasound irradiation

LETTERS IN ORGANIC CHEMISTRY(2011)

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摘要
A mild and efficient method for the chemoselective preparation of 1,1-diacetates catalyzed by 1-methyl-3-(3-sulfopropyl)-imidazolium methyl sulfate under ultrasound irradiation has been developed. The yields are ranged in 90% similar to 98%. This protocol offered several advantages including low catalyst loading, high yields, short reaction time and environmentally benign approach.
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关键词
1,1-diacetates,1-methyl-3-(3-sulfopropyl)-imidazolium methyl sulfate,aldehydes,catalyze,synthesis,ultrasound irradiation
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