Analysis of the unsaponifiable fraction of lipids belonging to various milk-types by using comprehensive two-dimensional gas chromatography with dual mass spectrometry/flame ionization detection and with the support of high resolution time-of-flight mass spectrometry for structural elucidation.

Peter Q Tranchida,Simona Salivo,Ivana Bonaccorsi,Archimede Rotondo,Paola Dugo,Luigi Mondello

Journal of Chromatography A（2013）

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摘要

•GC×GC–MS/FID was used for the analysis of the unsaponifiable fraction of milk lipids.•The structure of many constituents was confirmed by using GC–high resolution ToF MS.•Sensitivity and group-type patterns were the GC×GC characteristics most exploited.

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关键词

Comprehensive two-dimensional gas chromatography,High resolution time-of-flight mass spectrometry,Milk lipids,Butter,Unsaponifiable fraction

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