Studying Of Pysz And Fysz Turbine Blade Coatings By Small-Angle Neutron Scattering

We present here results of small-angle neutron scattering (SANS) investigation of partially and fully yttria stabilized zirconia (PYSZ and FYSZ, respectively) turbine blade coatings (TBC). The samples have been prepared by electron beam physical vapour deposition method (EB-PVD) with various setup parameters. Structure parameters of porosity have been studied in-situ with high-temperature furnace. Temperature dependence of specific surface and anisotropy parameter of porosity has been obtained. Differences in character of microstructural morphology changing with in-situ thermal treatment as well as open and closed porosity ratio in PYSZ and FYSZ has been described and discussed.