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Lattice Relations and Solidification of the Complex Regular Eutectic (Cr,fe)-(Cr,fe)(23)c-6

Metals and Materials International(2017)SCI 2区SCI 3区

Department of Materials Science and Engineering

Cited 2|Views10
Abstract
The eutectic (Cr,Fe)-(Cr,Fe)23C6 showed a triaxial fishbone structure and could be categorized as a “complex regular structure”. In this study, the lattice relations of the fishbone (Cr,Fe)23C6 were examined and the solidification process was observed using a transmission electron microscope and a confocal laser scanning microscope. For one of the three fish bones in a eutectic cell, parallel (Cr,Fe)23C6 lamellas at one side of the spine had the same lattice direction, as did those in the (Cr,Fe) phase. The lattices of neighboring (Cr,Fe)23C6 and (Cr,Fe) phases were not coherent. Lamellar (Cr,Fe)23C6 on opposite sides of a spine had different lattice directions, and their lattice boundary was in the spine. By using the confocal laser scanning microscope, the solidification of lamellar eutectic structure could be observed. At the low cooling rate of 5 o C·min-1, parallel lamellas would grow thick blocks instead of thin plates. To obtain a thin lamellar eutectic structure, the cooling rate should be higher, like the rate in welding.
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complex regular eutectic,(Cr,Fe)(23)C-6,confocal laser scanning microscope
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要点】:本文研究了复杂规则共晶(Cr,Fe)-(Cr,Fe)23C6的晶格关系及凝固过程,揭示了其独特的三轴鱼骨结构及其形成机制。

方法】:通过透射电子显微镜和共聚焦激光扫描显微镜对晶格关系进行观察,对凝固过程进行实时监测。

实验】:实验使用透射电子显微镜和共聚焦激光扫描显微镜对(Cr,Fe)23C6共晶的晶格关系和凝固过程进行研究,发现当冷却速度为5 o C·min^-1时,平行片层会形成厚块状结构,而要形成薄层共晶结构,则需要更高的冷却速率,如焊接过程中的冷却速率。