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Facile Preparation of Zno Particles with Different Structures and Their Photocatalytic Activity

World journal of engineering(2016)

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摘要
Purpose - This paper aims to report a novel preparation method of ZnO particles with different structures and their photocatalytic activity.Design/methodology/approach - ZnO powders are prepared by a facile, economical and environment-friendly aqueous solution route. X-ray diffraction, field emission scanning electron microscopy, energy dispersive spectroscopy, transmission electron microscopy and UV-vis diffuse reflectance spectra are used to characterize the products. Photocatalytic activity of the samples is evaluated by degradation of organic pollutant pentachlorophenol under UV-vis irradiation.Findings - It is found that three-dimensional ZnO hierarchical structures can be prepared via aqueous solution route without using any template or structure-directing agent, and the alkalinity of reaction solution is the key factor. All the as-prepared ZnO products have good catalytic activity under UV-vis light irradiation.Originality/value - This report presents a simple method for the preparation of ZnO particles with excellent photocatalytic activity. Experimental results could provide useful reference for the treatment of chlorophenols in the future.
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关键词
Preparation,ZnO,Hierarchical structure,Pentachlorophenol
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