Physical–chemical Analysis and Kinetics of the Magnetic Biocatalyst for 2,3,6,-Trimethylphenol Oxidation
Reaction kinetics, mechanisms and catalysis(2020)
摘要
In the paper, the synthesis of the magnetic biocatalyst based on immobilized peroxidase is described. This catalyst was tested in the reaction of 2,3,6,-trimethylphenol oxidation with the help of hydrogen peroxide to 2,3,5-trimethylhydrochinone (vitamin E intermediate). In the work, the method for magnetic nanoparticle synthesis was chosen. To characterize the synthesized biocatalyst physical–chemical analysis was carried out: transmission electron microscopy, FTIR spectroscopy, the study of magnetic characteristics with vibration magnetometer, X-ray photoelectron spectroscopy, low-temperature nitrogen adsorption. The optimum conditions for the process of 2,3,6,-trimethylphenol oxidation in the presence of magnetic biocatalyst (the substrate initial concentration, temperature, pH).
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关键词
Peroxidase,Immobilization,Magnetic nanoparticles,-Trimethylphenol,Oxidation
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