Catalytic Reductive Cleavage Of Poly(Phenylene Sulfide) Using A Hydrosilane

Yasunori Minami,Nao Matsuyama,Yasuaki Matsuo,Masanori Tamura,Kazuhiko Sato,Yumiko Nakajima

SYNTHESIS-STUTTGART（2021）

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摘要

The solvent-insoluble poly(phenylene sulfide) main chain was reductively cleaved by using triethylsilane as a hydrogen source under palladium/IcHex catalytic conditions. After the reaction, benzene and bis(triethylsilyl) sulfide as a sulfide source were formed efficiently. This method could be operated on a gram scale.

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关键词

palladium, polymer, reduction, silane, sulfur

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