Crystallization study of sol–gel derived 13-93 bioactive glass powder

Qaisar Nawaz,Araceli De Pablos-Martin,Juliana Martins De Souza E Silva,Lutz Berthold,Katrin Hurle,Altair T. Contreras Jaimes,Maciej Sitarz,Delia S. Brauer,Aldo R. Boccaccini

Journal of the European Ceramic Society（2021）

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摘要

•13–93 bioactive glass was synthesized via sol–gel method.•Crystallinity of 13–93 BG powder tailored in the range 5–43 wt.% by controlling heat treatment parameters.•TEM revealed the presence of different morphologies in the glass-ceramic microstructure as a function of heat treatment.•Nano-CT volumetric images showed the morphology and porosity of heated treated samples.

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关键词

Bioactive glasses,Sol–gel,Sintering of 13-93 bioactive glass,Crystallization behavior,Rietveld refinement

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