A Molecular “ A ‐Type” Tangled Metallocube

Li-Li Ma,Yang Li,Xin Li,Le Zhang,Li-Ying Sun,Ying-Feng Han

Angewandte Chemie（2022）

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摘要

A molecular “A-type” tangled metallocube has been generated by the reaction of a binuclear gold-N-heterocyclic carbene (NHC) complex and H2S. The tangled cube topology with 8 [(μ3-S)Au3]+ units and 12 bis-NHC ligands was validated by NMR spectroscopy, mass spectrometry, and single-crystal X-ray diffraction analysis.

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