Synthesis of phosphiranes via organoiron-catalyzed phosphinidene transfer to electron-deficient olefins

Tiansi Xin,Michael B. Geeson,Hui Zhu,Zheng-wang Qu,Stefan Grimme,Christopher Cummins

Chemical Science（2022）

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摘要

Herein is reported the structural characterization and scalable preparation of the elusive iron-phosphido complex FpP(tBu)(F) (2-F, Fp = (Fe(η5-C5H5)(CO)2)) and its precursor FpP(tBu)(Cl) (2-Cl) in 51% and 71% yields, respectively....

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