Good laboratory practice in thermal analysis and calorimetry

Journal of Thermal Analysis and Calorimetry(2023)

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摘要
During ICTAC2020, a workshop was held on “Good laboratory practice in thermal analysis and calorimetry” for young researchers and beginners under the aegis of the Education Committee of ICTAC. Thermal analysis (TA) covers relationship between large number of sample properties and the temperature. Naturally, there is some technique for each property of the sample bringing versatility in TA. This review is devoted to the Workshop and has been refined for the benefit of the readers so that it helps them in obtaining useful qualitative and quantitative information about the effects of heat treatments on materials of all kinds. Recent trends in DSC, TG-FTIR, TG-MS, DMA, kinetics and nanocalorimetry have also been covered in this article.
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关键词
DSC, Heat-flux DSC, Power-compensated DSC, Area under peak, Laboratory practice, Thermogravimetry, TG-FTIR, TG-MS, Materials, Dynamic mechanical analysis, Relaxation phenomena, Thermal analysis, Kinetics, Model-free methods, General rate equation, Nanocalorimetry, Ultrafast chip calorimetry, In situ experiments
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