Microwave Flow Chemistry: Single-mode System for Kg-Scale Organic Synthesis

Kohei Sato, Jun Ueda,Takuya Kon, Yushi Nakamura,Junko Fujimoto,Tetsuo Narumi,Kazuhiro Takeda,Nobuyuki Mase

2022 Asia-Pacific Microwave Conference (APMC)（2022）

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摘要

The optimization of single-mode microwave-assisted flow reaction conditions was investigated by improving sampling efficiency through microwave power gradients and in-line analysis, and advanced prediction through response surfaces. Application to kg-scale organic transformations highlights the utility of this protocol.

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关键词

microwave heating,optimization,flow reaction,in-line analysis,response surfaces

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