Microscopic Study of Shale Anisotropy with SEM In Situ Compression and Three-Point Bending Experiments

The microscopic anisotropy of shale has an important impact on its mechanical properties and crack behavior, so it is essential to understand the microscopic origin of anisotropic growth with a more effective laboratory work scheme. Uniaxial compression test and three-point bending test are considered to be efficient means to study the elastic properties and crack behavior of rocks. In this paper, uniaxial compression experiments and three-point bending experiments were conducted on shale outcrops in the Changqing area using field emission scanning electron microscopy (SEM) and in situ tensile testing, and the microscopic deformation and crack processes were quantitatively characterized by the digital image correlation (DIC) method. For the compression experiments, the observation of the first principal strain fields indicated that the microscopic anisotropy of shale was related to the bedding planes, and the microscopic deformations were mainly concentrated in the clay mineral accumulation area and at the microcracks. Elastic moduli and compressive strengths of specimens with different bedding angles were affected by the strong shear stress effects. The specimens with a bedding angle of 30 degrees showed lower peak loads and compressive strengths, and the specimens with a bedding angle of 60 degrees had lower elastic moduli. Three-point bending experiments were conducted for studying the effects of crack-bedding orientation relationships on cracking processes, and four critical fracturing mechanical properties were calculated. The short transverse-type cases were prone to break and had a lower peak load, tensile strength, fracture toughness and elastic-bending modulus. The divider-type cases were more difficult to break, formed a more tortuous crack and had a higher tensile strength, fracture toughness and elastic-bending modulus. The arrester-type cases had a middle range of mechanical parameters but developed the longest cracks. This study provides a feasible experimental and analysis method for understanding the microscopic anisotropy of shale samples. The small specimen size also makes the requirements of core samples easier to be satisfied considering the field application. Furthermore, the anisotropy of cracking processes can be understood better by building the connections between microstructural characteristics and mechanical performances.