Effect of Subcritical ? Solution Treatment on the Primary a Phase, Element Partitioning and Aging Precipitation of TB17 Titanium Alloy
RARE METAL MATERIALS AND ENGINEERING(2023)
摘要
Subcritical ss solution treatment of TB17 titanium alloy was carried out at the solution temperature range from 800 degrees C to 835 degrees C and the solution time range from 0.5 h to 9 h, and the distribution of Al, Mo and Nb elements in the primary a phase, element partitioning and ss matrix was studied by electron probe microanalysis (EPMA). Effect of subcritical ss solution on precipitation of primary a phase and secondary a phase of the alloy was investigated. The experimental results show that primary a phase presents two typical morphologies of needle- type and lamellae-type structure, which the needle-type a phase is distributed at grain interior and lamellae-type a phase is distributed at grain boundaries. The amount of primary a phase decreases with the increasing of solution temperature. No primary a phase is observed at the solution temperature higher than 825 degrees C. The amount of primary a phase increases with the decreasing of solution temperature. The precipitation of primary a phase will reach a steady state at the temperature of 815 degrees C and the solution time higher than 2 h. Al element tends to be enriched in the primary a phase, and Mo and Nb elements tend to be enriched in the ss matrix. The Al concentration in the center of the a phase is higher than that in the edge, while the Mo and Nb concentration in the center is lower than that in the edge. Increasing the amount of primary a phase will decrease Al concentration and increase Mo and Nb concentration in the ss matrix. When the amount of primary a phase is low, the secondary a phase near primary a phase presents the morphologies of needle-type or lamellae- type structure, and morphology of the basketweave structure for the secondary a phase far from primary a phase. When the amount of primary a phase is high, the secondary a phase presents the morphologies of needle-type or lamellae-type structure.
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关键词
TB17 titanium alloy,subcritical ss solution treatment,primary a phase,element partitioning,aging precipitation
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