Fe^III/TBHP mediated remote C–O bond construction of 8-aminoquinolines: access to methoxylation and cyanomethoxylation

Mengfei Zhao,Kaixin Zhang,Jianxiong Xu,Jizhen Li

Organic Chemistry Frontiers（2022）

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摘要

The C5 regioselective methoxylation and cyanomethoxylation of 8-aminoquinolines were achieved under FeIII/TBHP system by tuning the temperature and solvent. TBHP was investigated as an “oxygen” source in the ether bond formation for the first time.

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FeIII/TBHP mediated remote C–O bond construction of 8-aminoquinolines: access to methoxylation and cyanomethoxylation

Fe^III/TBHP mediated remote C–O bond construction of 8-aminoquinolines: access to methoxylation and cyanomethoxylation