Synthesis, optical properties and crystal structure of (E,E)-1,3-(3,4:9,10-dibenzododeca-1,11-diene-5,7-diyne-1,12-diyl)benzene

Hikaru Watanabe,Takuma Sato,Michiki Sumita,Mei Shiroyama,Daichi Sugawara,Tomoki Tokuyama,Yasuhiro Okuda,Kan Wakamatsu,Haruo Akashi,Akihiro Orita, S. Parkin

Acta crystallographica. Section E, Crystallographic communications（2023）

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摘要

A dehydrobenzannulene, (E,E)-1,3-(3,4:9,10-dibenzododeca-1,11-diene-5,7-diyne-1,12-diyl)benzene, was stereoselectively synthesized, and its crystal structure and UV-Vis absorption and photoluminescence optical properties were determined.

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关键词

crystal structure,expanded π-system,dehydrobenzannulene,reductive desulfonylation

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Synthesis, optical properties and crystal structure of (E,E)-1,3-(3,4:9,10-dibenzododeca-1,11-diene-5,7-diyne-1,12-di­yl)benzene

Synthesis, optical properties and crystal structure of (E,E)-1,3-(3,4:9,10-dibenzododeca-1,11-diene-5,7-diyne-1,12-diyl)benzene