Rh(III)-Catalyzed Direct ortho Alkylation of Carbazoles with Nitroalkenes

Liming Zhang, Ru Zhao, Chunhui Liu, Zhaoyang Li,Jun-Long Niu,Hao-Ran Yang,Lijun Gao,Shuang-Liang Liu,Liming Zhou

ADVANCED SYNTHESIS & CATALYSIS（2023）

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摘要

The Rh(III)-catalyzed ortho alkylation of N-pyridylcarbazoles with nitroalkenes has been developed, furnishing a wide range of 2-(2nitroalkyl)carbazoles. Both aromatic and aliphatic nitroalkenes participated in this alkylation reaction successfully. This protocol also proceeded well with an indoline based substrate. Derivatization of the representative nitroalkane product was described.

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关键词

carbazole,nitroalkene,alkylation,rhodium,C-H activation

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