Pushing the limits of sensitivity and resolution for natural abundance ⁴³Ca NMR using ultra-high magnetic field (35.2 T)

Christian Bonhomme, Xiaoling Wang,Ivan Hung,Zhehong Gan,Christel Gervais,Capucine Sassoye,Jessica Rimsza,Jincheng Du,Mark E. Smith,John V. Hanna,Stéphanie Sarda,Pierre Gras,Christèle Combes,Danielle Laurencin

Chemical Communications（2018）

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摘要

Natural abundance 43Ca solid state NMR experiments are reported for the first time at ultra-high magnetic field (35.2 T) on a series of Ca-(pyro)phosphate and Ca-oxalate materials, which are of biological relevance in relation to biomineralization processes and the formation of pathological calcifications.

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Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T)

Pushing the limits of sensitivity and resolution for natural abundance ⁴³Ca NMR using ultra-high magnetic field (35.2 T)