Synergistic interfacial effects of sizing agent containing gradient curing agent and pre-heating treated carbon fibers
COMPOSITES SCIENCE AND TECHNOLOGY(2024)
摘要
This investigation focuses on the use of sizing agent containing gradient curing agent from two directions for carbon fibers coupled with pre-heating treatment before fibers combined into composites to improve interfacial adhesion. Growth in interfacial shear strength (IFSS) up to 92.4 % was noticed for fibers functionalized with sizing agent of high-to-low curing agent from fiber-to-resin (CFH -> L), relative to control fibers. This is related to the greatly enhanced interactions at both fiber/sizing and sizing/resin interfaces accompanied by increased interfacial curing degree that generate a stronger interphase. Further optimization of 4.1 % increase in IFSS was achieved for CFH -> L via pre-heating treatment before being composites, while larger IFSS increment of 16.7 % after pre-heating treatment was observed for fibers coated with sizing agent of low-to-high curing agent from fiber-to-resin (CFL -> H). This reveals that pre-heating is more effective for fiber that has weaker interactions with sizing agent. This work is believed to be a preliminary but crucial trial toward obtaining high-performance fiber composites by simply applying it in the already existed fiber production line.
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关键词
Carbon fibers,Polymer -matrix composites (PMCs),Fibre/matrix bond,Interphase
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