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Effect of Microalloying with Rare-Earth Lanthanum on Dynamic Recrystallization Behavior and Mechanical Properties of Ti Sheets

Materials today. Communications(2024)

Cent South Univ

Cited 0|Views15
Abstract
This study examines the influence of microalloying with rare earth lanthanum (La) on the dynamic recrystallization behavior and mechanical properties of Titanium (Ti) sheets. A distinctive wedge-shaped specimen was employed for experimental efficiency, enabling continuous gradient strains to be applied to the Ti-La alloy during hot-rolling, facilitating the assessment of changing microstructural, textural, and hardness features as strain increased from low to high levels. The hot-rolled plates were performed using analytical methods such as optical microscopy (OM), X-ray diffraction (XRD), transmission electron microscopy (TEM), and hardness testing. The results show that the hardening process can be divided into four stages under continuous gradient strain (0 ~ 0.5, 0.5 ~ 0.7, 0.7 ~ 1.2 and 1.2 ~ 1.6). During these stages, grain refinement and dislocation strengthening emerge as critical contributors to changes in hardness. Furthermore, it was determined that dynamic recrystallisation (DRX) of Ti-La alloys during hot rolling occurs at the fourth stage. Analysis of the orientation distribution function (ODF) reveals that the dominant textures during this process include {1̅21̅0}, {011̅0}, and {0001} textures. When compared with commercially pure titanium (CP-Ti), the Ti-La alloy shows significantly delayed DRX under identical conditions. The DRX grain growth appears suppressed, attributable to the presence of La-rich particles on the grain boundaries. Moreover, the texture associated with rolling deformation seems subdued, providing a desirable base for future cold rolling and heat treatment.
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Key words
Titanium alloy,Lanthanum addition,Hot rolling,Microstructure and texture,Mechanical properties
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要点】:本研究探讨了微合金化添加稀土元素镧(La)对钛(Ti)板材动态再结晶行为和机械性能的影响,发现La的添加显著延迟了动态再结晶并改善了机械性能。

方法】:通过使用独特的楔形试样,在热轧过程中对Ti-La合金施加连续梯度应变,采用光学显微镜(OM)、X射线衍射(XRD)、透射电子显微镜(TEM)和硬度测试等方法进行实验分析。

实验】:通过热轧实验,分析不同应变阶段下Ti-La合金的微结构、织构和硬度特征,发现动态再结晶发生在第四阶段,且与商业纯钛(CP-Ti)相比,Ti-La合金在相同条件下动态再结晶明显延迟,晶粒长大受到抑制,且滚动变形纹理减弱,有利于后续冷轧和热处理。数据集名称未明确提及。