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1Synthesis of Heterocyclic Azoxy Compounds from C-Nitroheterocyclic Compounds and Metal Derivatives of Tert-Butylamine

É. T. Apasov,E. V. Shepelev,B. A. Dzhetigenov,Yu. A. Strelenko,A. V. Kalinin,V. A. Tartakovskii

The reaction of 3-nitropyrazole and 3(5)-nitro-1,2,4-triazole with t-BuNHMgBr gives the corresponding asymmetrical diazene oxides. Furthermore, 3(5)-(1,1-dimethylethyl)azoxy-1,2,4-triazole was also synthesized by the reaction of 1-trimethylsilyl-3(5)-nitro-1,2,4-triazole with t-BuNHLi.

1994ChemInform（1994）引用：1

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2Peculiarities of the Interaction of Dinitrobenzenes with T-Bunhmgbr and T-Bunhli

E. T. Apasov,B. A. Dzhetigenov,E. V. Shepelev,Yu. A. Strelenko,A. V. Kalinin

Reactions of m- and p-dinitrobenzenes with t-BuNHMgBr and t-BuNHLi were studied. The reactions afford azo- and azoxy-derivatives and products of nucleophilic substitution.

1993Russian chemical bulletin（1993）引用：2

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3ChemInform Abstract: N‐Lithiated Derivatives of Aliphatic Amines in the Synthesis of 1‐ Alkyl‐2‐phenyldiazene 2‐Oxides.

E. V. SHEPELEV,N. N. KOSTIKOVA,B. A. DZHETIGENOV,A. V. KALININ

AbstractChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.

1992引用：1

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4N-Lithium Derivatives of Aliphatic-Amines in the Synthesis of 1-Alkyl-2-phenyldiazene 2-Oxides

E. V. Shepelev,N. N. Kostikova,B. A. Dzhetigenov,A. V. Kalinin

Magnesium derivatives of aliphatic amines containing α-hydrogen atoms, in contrast to t-BuNHMgBr, do not form phenylaliphatic diazene oxides upon reaction with nitrobenzene, but rather reduce it to azobenzene and azoxybenzene. Asymmetric diazene oxides are formed when the magnesium derivatives are replaced by lithium derivatives. The reaction of t-BuNHLi with dimethylnitramine gives 1,3,5-trimethyl-1,3,5-triazacyclohexane.

1991Bulletin of the Academy of Sciences of the USSR Division of Chemical Science（1991）引用：1

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5ChemInform Abstract: DAS VERH. VON TRIS‐ACETYLAMINO‐METHAN IN TRIFLUORESSIGSAEURE

G. A. KALABIN, S. N. SHEDOVA,E. V. SHEPELEV,O. V. LEBEDEV,L. I. KHMEL'NITSKII,S. S. NOVIKOV

Chemischer InformationsdienstVolume 3, Issue 15 Preparative Organic Chemistry ChemInform Abstract: DAS VERH. VON TRIS-ACETYLAMINO-METHAN IN TRIFLUORESSIGSAEURE G. A. KALABIN, G. A. KALABINSearch for more papers by this authorS. N. SHEDOVA, S. N. SHEDOVASearch for more papers by this authorE. V. SHEPELEV, E. V. SHEPELEVSearch for more papers by this authorO. V. LEBEDEV, O. V. LEBEDEVSearch for more papers by this authorL. I. KHMEL'NITSKII, L. I. KHMEL'NITSKIISearch for more papers by this authorS. S. NOVIKOV, S. S. NOVIKOVSearch for more papers by this author G. A. KALABIN, G. A. KALABINSearch for more papers by this authorS. N. SHEDOVA, S. N. SHEDOVASearch for more papers by this authorE. V. SHEPELEV, E. V. SHEPELEVSearch for more papers by this authorO. V. LEBEDEV, O. V. LEBEDEVSearch for more papers by this authorL. I. KHMEL'NITSKII, L. I. KHMEL'NITSKIISearch for more papers by this authorS. S. NOVIKOV, S. S. NOVIKOVSearch for more papers by this author First published: April 11, 1972 https://doi.org/10.1002/chin.197215164Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat No abstract is available for this article. Volume3, Issue15April 11, 1972 RelatedInformation

1972

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6Structure of Condensation Product of Ethyl Orthoformate with Acetamide

S. S. Novikov,L. I. Khmel'nitskii,S. N. Shvedova,E. V. Shepelev,O. V. Lebedev

Independent of the reaction conditions employed, trisacetylaminomethane is formed when ethyl orthoformate is reacted with acetamide.

1971Bulletin of the Academy of Sciences of the USSR, Division of chemical science（1971）

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7Behavior of Trisacetylaminomethane in Trifluoroacetic Acid

G. A. Kalabin,S. N. Shvedova,E. V. Shepelev,O. V. Lebedev,L. I. Khmel'nitskii,S. S. Novikov

A study was made of the behavior of trisacetylaminomethane in trifluoroacetic acid.

1971Bulletin of the Academy of Sciences of the USSR, Division of chemical science（1971）

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8ChemInform Abstract: UEBER DIE STRUKTUR DES KONDENSATIONSPRODUKTS AUS AETHYL‐ORTHOFORMIAT UND ACETAMID

S. S. NOVIKOV,L. I. KHMEL'NITSKII,S. N. SHVEDOVA,E. V. SHEPELEV,O. V. LEBEDEV

AbstractIn früheren Arbeiten wird angegeben, daß bei der Umsetzung von Orthoameisensäureester (I) mit 3 Mol Acetamid (II) Tris‐acetylamino‐methan (III)‐, unter etwas geänderten Bedingungen (ohne Lösungsmittel und ohne Katalysator) N,N′‐Diacetyl‐formamidin (IV), bzw. beim Verhältnis (I):(II) = l:0,2 bis 1,5 Äthyl‐N‐acetyl‐formimidat (V) entstehen.

1971Chemischer Informationsdienst Organische Chemie

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9Structure Of Product Resulting From Condencation Of Ethyl Orthoformate With Acctamide