Terrestrial shale strata generally has frequent and strong heterogeneity characteristics, thus affecting shale gas enrichment and target selection. In this study, samples from the Da’anzhai Member of Well A in Yuanba area have performed a series of experiments including total organic carbon ( TOC ) content measurement, rock pyrolysis, organic petrology, vitrinite reflectance ( R o ), whole-rock mineral composition, thin section analysis, focused ion beam scanning electron microscope, high-pressure Hg injection, nitrogen (N 2 ) adsorption, and methane (CH 4 ) isothermal adsorption. The results show that: (1) Da'anzhai (J 1 da) Member is a set of mixed sediments with various lithology, which consists of black shale and well-developed siltstone and carbonate rocks interlayers. The second section of the Da'anzhai Member (J 1 da 2 ) has relatively greater organic matter abundance (1.24% TOC ), better organic matter type dominated by type III and II, as well as higher maturity (1.67% R o ), which is the most favorable section of J 1 da. (2) J 1 da 2 shale strata can be divided into three shale lithofacies types, two interlayer lithofacies types, and three macro-lithofacies assemblage types. Among them, mudstone–limestone lithofacies assemblage (type AB-I) has preferable hydrocarbon generation conditions, better reservoir properties, and more developed shell limestone interlayers with better fracturing performance, is thought the most favorable interval. (3) The optimal interval and horizontal target of J 1 da 2 are further selected based on the source–reservoir coupling relationship, corresponding to the depth is 3909–3914 m, which imply the optimal horizontal target window for Well A. This study has application values not only for the identification of “sweet intervals” and well location deployment of J 1 da but also supports the later systematic studies of shale gas accumulation mechanism and enrichment regularity in Yuanba area.
Rock pyrolysis, organic petrology, vitrinite reflectance, gas chromatography-mass spectrometry (GC-MS) analysis, and biomarker compound analysis were performed to comprehensively analyze the organic geochemical characteristics of the Jurassic Da’anzhai Member (J 1 da) shale strata in Yuanba and Puguang areas in the northeastern Sichuan Basin. Then the organic matter provenance and sedimentary environment were further analyzed. Finally, the significance of oil and gas exploration in J 1 da shale strata was discussed. Results show that the second section of the Da’anzhai Member (J 1 da 2 ) has relatively high organic matter abundance (1.24% TOC ), type Ⅱ-dominated organic matter type, which is the most favorable section of wells Y1 and T1 in the study area. The organic matter maturity and the hydrocarbon phases are quite different, which is 1.01% R o dominated by oil generation in Puguang area, while it is 1.67% R o dominated by gas generation in Yuanba area. Content and chromatograms of biomarkers including n-alkanes, tricyclic terpanes, C 24 tetracyclic terpanes, and C 27 -C 28 -C 29 regular steranes show that the organic matters of J 1 da shale strata derive from both terrestrial higher plants and lower aquatic organisms, with slightly differentiated mixed ratio of each sublayer. Characteristics of Pr/Ph, γ-cerane and hopanes compounds indicate that the overall depositional environment of J 1 da is a freshwater lacustrine environment, with saline lake deposits in local areas and intervals in the study area. The rapid changes of sedimentary environment have resulted in obvious stratification of water body, frequent interbeds, and strong heterogeneity of J 1 da shale strata. Comprehensive analysis shows the shale/mud microfacies in the semi-deep lake subfacies and shale/mud interbedded with siltstone and shell bank microfacies in the shallow lake subfacies are the most favorable sedimentary facies for J 1 da hydrocarbon enrichment. Deeper burial depth and higher maturity make for oil and gas enrichment with higher gas/oil ratio (GOR); moreover, the thicker intervals with organic-rich shale are favorable targets for geochemical evaluation.