The applications of adaptive optics extend across multiple sectors, encompassing areas such as LiDAR, biological and chemical sensing, and free-space communications. In this study, we report on the design, fabrication, testing, and modeling of electrically reconfigurable metasurfaces using a low-loss high contrast phase change material, Ge2Sb2Se4Te integrated with an IR-transparent silicon microheater. Through this work, we introduce a reliable architecture for switching PCM-based metasurfaces within an integrated circuit configuration and the capability of controlling the transmission of electromagnetic waves through the precise stimulation of PCM-based pixels, each spanning a few hundred microns, over numerous cycles. By leveraging PCM-based pixels, we unlock the potential to create metasurfaces encompassing a diverse range of functionalities such as dielectric filters, metalens, or beam steering devices, which is governed by the design of the meta-atoms.

We report the results of the effect of prolonged low-Earth orbit exposure on phase-change materials (PCMs) and PCM-based metasurfaces. During a 6-month exposure as part of the Materials on the International Space Station Experiment (MISSE-14) test campaign led by NASA Langley Research Center, Ge2Sb2Te5 (GST) and GST-based metasurface spectral filters were monitored for their response to extreme temperature cycles, UV and ionizing radiation fluences, and atomic oxygen fluences. Upon return to Earth, the samples were characterized and compared to their pre-flight condition to glean insight into the effects of the space environment on metasurface performance and PCM optical and structural properties.

We report the design, fabrication, and testing of electrically tunable metasurface k-space filters based on the phase-change material GSST and a transparent Si electrode heating architecture. A 10x10 array of PCM elements and Si heaters was fabricated via the foundry processes, and used to control the crystallinity of a metasurface consisting of GSST nano antennae. By selectively crystallizing individual elements, specific k-vectors of transmitted light can effectively be filtered out, resulting in improved imaging quality by reducing the scattered light that reaches the detector. Optimized doping profiles in the Si heaters allow for uniform, low power switching of the GSST state.

Optical metasurfaces are planar subwavelength nanoantenna arrays engineered to provide on-demand manipulation of light, thereby enabling ultra-compact flat optics with high performance, small form-factor and new functionalities. When integrated with active elements, the pixelated, thin device architecture further facilitates dynamic tuning of local and global optical responses. Leveraging advanced materials, designs and architectures, we develop novel active and passive meta-optics capable of transforming a variety of optical systems that are traditionally bulky and complicated.

Phase change material (PCM)-based actively tunable mid-wave IR filters have broad imaging and sensing applications—from probing molecular vibrations in chemical species to detecting radiant thermal signatures. We introduce the Phase-change actively tunable filter (P-ACTIVE) project lead by NASA Langley Research Center with collaborators MIT and the University of Cambridge. It covers background science, experimental and theoretical device performance, as well as recent results obtained from a MISSE-14 mission for space qualification of active metasurface optics and constituent PCM. We conclude with a prospective view of the technology and discuss the potential for these filters to serve multiple NASA missions.

In this work, we introduce actively tunable PCM-FP (Fabry-Perot) and PCM-PNA (Plasmonic Nanohole Array) bandpass filters that possess high-speed tunability (MHz), narrow spectral bandwidth, high-transmissivity, broad tuning range, in an all solid-state design in a wide variety of imaging and spectroscopic applications. We also present the results from a Materials International Space Station Experiment (MISSE-14) in which chalcogenide phase change material (PCM) optical components are exposed and tested in Low Earth Orbit to determine their suitability for space applications. Our samples including Ge2Sb2Te5, Ge2Sb2Se4Te1, Sb2S3 thin-films and PCM-FP were delivered aboard the ISS by Northrop Grumman (NG-15) in Feb. 2021 for 6 months of exposure testing, including: temperature, vacuum, atomic oxygen, UV exposure and solar illumination effects. Our MISSE-14 PCM study will provide valuable information on the limitations and suitability of PCMs in harsh space environments.

The mid-wave infrared (MWIR) waveband (3-5 µm) contains numerous invaluable spectral /thermal signatures. Tunable MWIR filters are thus highly desirable in a variety of imaging and spectroscopic applications. We introduce phase-change tunable filters (PCTFs) which enable actively tunable spectral filtering across the MWIR waveband from a single solid-state element. This is achieved through the integration of the chalcogenide phase-change material GeSbTe (GST) into a plasmonic nanohole metasurface. We demonstrate polarization-insensitive PCTFs with >70% transmittance, 60nm bandwidth, and high-speed switching (MHz-GHz) across the MWIR waveband using a nanosecond laser pulse. We further show PCTF-based multispectral thermal imaging and dynamic gas sensing.

Tunable mid-wave infrared (MWIR) filters are highly desirable in a wide variety of imaging and spectroscopic applications; with the waveband containing numerous invaluable spectral absorption signatures. We demonstrate spectrally-tunable, all solid-state, thin-film bandpass filters operating across the MWIR by utilizing the phase-change material (PCM) Ge2Sb2Te5 as a tunable cavity medium between two Bragg mirrors. The induced PCM refractive index modulation increases the cavity’s optical path length, thereby tuning the filter passband. Our filters have 300 nm spectral tunability, ~70% transmission efficiencies, and ~60 nm passbands. We further show multispectral thermal imaging and dynamic CO2 gas plume sensing using the filters.

Actively tunable optical filters based on chalcogenide phase-change materials (PCMs) are an emerging technology with applications across chemical spectroscopy and thermal imaging. The refractive index of an embedded PCM thin film is modulated through an amorphous-to-crystalline phase transition induced through thermal stimulus. Performance metrics include transmittance, passband center wavelength (CWL), and bandwidth; ideally monitored during operation (in situ) or after a set number of tuning cycles to validate real-time operation. Measuring these aforementioned metrics in real-time is challenging. Fourier-transform infrared (IR) spectroscopy provides the gold-standard for performance characterization yet is expensive and inflexible—incorporating the PCM tuning mechanism is not straightforward, hence in situ electro-optical measurements are challenging. In this work, we implement an open-source MATLAB®-controlled real-time performance characterization system consisting of an inexpensive linear variable filter (LVF) and mid-wave IR camera, capable of switching the PCM-based filters while simultaneously recording in situ filter performance metrics and spectral filtering profile. These metrics are calculated through pixel intensity measurements and displayed on a custom-developed graphical user interface in real-time. The CWL is determined through spatial position of intensity maxima along the LVF's longitudinal axis. Furthermore, plans are detailed for a future experimental system that further reduces cost, is compact, and utilizes a near-IR camera.

Tunable narrowband spectral filtering across arbitrary optical wavebands is highly desirable in a plethora of applications, from chemical sensing and hyperspectral imaging to infrared astronomy. Yet, the ability to reconfigure the optical properties, with full reversibility, of a solid-state large-area narrowband filter remains elusive. Existing solutions require either moving parts, have slow response times, or provide limited spectral coverage. Here, we demonstrate a 1-inch diameter continuously tunable, fully reversible, all-solid-state, narrowband phase-change metasurface filter based on a GeSbTe-225 (GST)-embedded plasmonic nanohole array. The passband of the presented device is ∼ 74 n m with ∼ 70 % transmittance and operates across the 3–5 µm thermal imaging waveband. Continuous, reconfigurable tuning is achieved by exploiting intermediate GST phases via optical switching with a single nanosecond laser pulse, and material stability is verified through multiple switching cycles. We further demonstrate multispectral thermal imaging in the mid-wave infrared using our active phase-change metasurfaces. Our results pave the way for highly functional, reduced power, compact hyperspectral imaging systems and customizable optical filters for real-world system integration.

We demonstrate spectrally-tunable Fabry-Perot bandpass filters operating across the MWIR by utilizing the phase-change material GeSbTe (GST) as a tunable cavity medium between two (Ge:Si) distributed Bragg reflectors. The induced refractive index modulation of GST increases the cavity’s optical path length, red-shifting the passband. Our filters have spectral-tunability of ∼300 nm, transmission efficiencies of 60-75% and narrowband FWHMs of 50-65 nm (Q-factor ∼70-90). We further show multispectral thermal imaging and gas sensing. By matching the filter’s initial passband to a CO2 vibrational-absorption mode (∼4.25 µm), tunable atmospheric CO2 sensing and dynamic plume visualization of added CO2 is realized.

Actively tunable, narrowband spectral filtering across arbitrary optical wavebands is highly desirable in a plethora of applications, from chemical sensing, hyperspectral imaging to infrared astronomy. Yet, the ability to actively reconfigure the optical properties of a solid-state narrowband filter remains elusive. Existing solutions require either moving parts, have slow response times or provide limited spectral coverage. Here, we demonstrate a continuously tunable, spectrally-agnostic, all-solid-state, narrowband phase-change metasurface filter based on a GeSbTe (GST)-embedded plasmonic nanohole array. The passband of the presented tunable filter is ~74 nm with ~70% transmittance and operates across 3 - 5 $\mu$m; the thermal imaging waveband. Continuous, reconfigurable tuning is achieved by exploiting intermediate GST phases via optical switching with a single nanosecond laser pulse and material stability is verified through multiple switching cycles. We further demonstrate multispectral thermal imaging in the mid-wave infrared using our phase-change metasurfaces. Our results pave the way for highly functional, reduced power, compact hyperspectral imaging systems and optical filters.

This paper provides an overview of recent wind tunnel tests performed at the NASA Langley Research Center where the Background-Oriented Schlieren (BOS) technique was used to provide information pertaining to flow-field density disturbances. The facilities in which the BOS technique was applied included the National Transonic Facility (NTF), Transonic Dynamics Tunnel (TDT), 31-Inch Mach 10 Air Tunnel, 15-Inch Mach 6 High-Temperature Air Tunnel, Rotor Test Cell at the 14 by 22 Subsonic Tunnel, and a 13-Inch Low-Speed Tunnel.

Visualization of the flow field around a generic re-entry capsule in subsonic flow and shock wave visualization with cylindrical explosives have been conducted to demonstrate sensitivity and applicability of background-oriented schlieren (BOS) for field experiments. The wind tunnel experiment suggests that BOS with a fine-pixel imaging device has a density change detection sensitivity on the order of 10(sup -5) in subsonic flow. In a laboratory setup, the structure of the shock waves generated by explosives have been successfully reconstructed by a computed tomography method combined with BOS.

This paper presents the results of visualization of separated flow around a generic entry capsule that resembles the Apollo Command Module (CM) and the Orion Multi-Purpose Crew Vehicle (MPCV). The model was tested at flow speeds up to Mach 0.4 at a single angle of attack of 28 degrees. For manned spacecraft using capsule-shaped vehicles, certain flight operations such as emergency abort maneuvers soon after launch and flight just prior to parachute deployment during the final stages of entry, the command module may fly at low Mach number. Under these flow conditions, the separated flow generated from the heat-shield surface on both windward and leeward sides of the capsule dominates the wake flow downstream of the capsule. In this paper, flow visualization of the separated flow was conducted using the background-oriented schlieren (BOS) method, which has the capability of visualizing significantly separated wake flows without the particle seeding required by other techniques. Experimental results herein show that BOS has detection capability of density changes on the order of 10(sup-5).

Planar laser-induced fluorescence (PLIF) flow visualization has been used to investigate the hypersonic flow of air over surface protrusions that are sized to force laminar-toturbulent boundary layer transition. These trips were selected to simulate protruding Space Shuttle Orbiter heat shield gap-filler material. Experiments were performed in the NASA Langley Research Center 31-Inch Mach 10 Air Wind Tunnel, which is an electrically-heated, blowdown facility. Two-mm high by 8-mm wide triangular and rectangular trips were attached to a flat plate and were oriented at an angle of 45 degrees with respect to the oncoming flow. Upstream of these trips, nitric oxide (NO) was seeded into the boundary layer. PLIF visualization of this NO allowed observation of both laminar and turbulent boundary layer flow downstream of the trips for varying flow conditions as the flat plate angle of attack was varied. By varying the angle of attack, the Mach number above the boundary layer was varied between 4.2 and 9.8, according to analytical oblique-shock calculations. Computational Fluid Dynamics (CFD) simulations of the flowfield with a laminar boundary layer were also performed to better understand the flow environment. The PLIF images of the tripped boundary layer flow were compared to a case with no trip for which the flow remained laminar over the entire angle-of-attack range studied. Qualitative agreement is found between the present observed transition measurements and a previous experimental roughness-induced transition database determined by other means, which is used by the shuttle return-to-flight program.

As part of a strategic, multi-facility test program, subscale testing of NASA s Crew Exploration Vehicle was conducted in both legs of NASA Langley s Unitary Plan Wind Tunnel. The objectives of these tests were to generate aerodynamic and surface pressure data over a range of supersonic Mach numbers and reentry angles of attack for experimental and computational validation and aerodynamic database development. To provide initial information on boundary layer transition at supersonic test conditions, transition studies were conducted using temperature sensitive paint and infrared thermography optical techniques. To support implementation of these optical diagnostics in the Unitary Wind Tunnel, the experiment was first modeled using the Virtual Diagnostics Interface software. For reentry orientations of 140 to 170 degrees (heat shield forward), windward surface flow was entirely laminar for freestream unit Reynolds numbers equal to or less than 3 million per foot. Optical techniques showed qualitative evidence of forced transition on the windward heat shield with application of both distributed grit and discreet trip dots. Longitudinal static force and moment data showed the largest differences with Mach number and angle of attack variations. Differences associated with Reynolds number variation and/or laminar versus turbulent flow on the heat shield were very small. Static surface pressure data supported the aforementioned trends with Mach number, Reynolds number, and angle of attack.

Two optically based flame-detection systems have been developed for use in NASA Langley's 8-Foot High-Temperature Tunnel (8-ft HTT). These systems are used to detect the presence and stability of the main-burner and pilot-level flames during facility operation. System design considerations will be discussed, and a detailed description of the system components and circuit diagrams will be provided in the Appendices of this report. A more detailed description of the manufacturing process used in the fabrication of the fiber-optic probes is covered in NASA TM-2001-211233.

This paper documents the design and development of the fiber-optic probes utilized in the flame detection systems used in NASA Langley Research Center''s 8-Foot High Temperature Tunnel (8-ft HTT). Two independent flame detection systems are utilized to monitor the presence and stability of the main-burner and pilot-level flames during facility operation. Due to the harsh environment within the combustor, the successful development of a rugged and efficient fiber-optic probe was a critical milestone in the development of these flame detection systems. The final optical probe design for the two flame detection systems resulted from research that was conducted in Langley''s 7-in High Temperature Pilot Tunnel (7-in HTT). A detailed description of the manufacturing process behind the optical probes used in the 8-ft HTT is provided in Appendix A of this report.